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Excerpt
from the technical equipment at the FIB

1. Analysis
and test equipment
1.1 Scanning electron microscopy
- Nova NanoSEM 230(Field emission
low vacuum - Scanning electron microscope (FEI Company)
with an analytic unit, consisting of
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Nova NanoSEM 230
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x-ray microanalysis (chemical information)
in combination with a Electron Backscattered Diffraction system (EBSD - crystallographic information) with
the name EDAX Pegasus XM 4 as well as a
cryo-work station, consisting of a high pressure freezing unit HPM 100 (Fa. BAL-TEC/Leica)
- PhilipsPhilips Environmental
Scanning Electron Microscope (XL-30 ESEM) with integrated
x-ray microanalysis system
- scanning electron microscope
Typ HITACHI S 2700LB (manufacturer: Hitachi,Tokyo) with EDS TRACOR Voyager 2100
with digital beam regulation and imaging system for SEM and EDX
and ESMA (manufacturer: Noran Instruments, USA)
1.2 Fine structure analysis
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XRD D8 ADVANCE
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- X-ray-generator Kristalloflex
710 D and X-ray-diffractometer D 5000 with automatic sample change,
high- and low temperature chamber, as well as moisture chamber (manufacturer: Siemens AG, Karlsruhe)
- X-ray diffractometer D8 ADVANCE (Bruker AXS),
new generation
- ORBIS PC Micro EDXRF Spectrometer System
(Fa. EDAX AMETEK Materials Analysis Division, USA)
- surface measuring instrument
ASAP 2000 (manufacturer: Micromeritics GmbH, Mönchengladbach) to the determination
the specific surface
- mercury intrusion porosimeter (MIP)
AUTOPORE IV 9500 (manufacturer Micromeritics GmbH,
Mönchengladbach) determination of the pore size distribution in mineral materials
- helium comparison pycnometer
SY-LAB ( manufacturer: Micromeritics GmbH, Mönchengladbach) for the determination of pure densities
at powder preparations
- automatical Blain-value-device
BLAINE-STAR ZEB 1330 (manufacturer: Wasagchemie Sythen GmbH) for the determination of
the specific surface of disperse solid materials
1.3 Thermal analysis
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Simultaneous DTA SDT (DSC-TGA)
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- simultaneous- thermoanalysis device
STA 409 for DTA-/DSC-measurements (manufacturer: Netzsch,
Selb)
- Isothermal heat flow calorimeter
ToniCAL TRIO Bauform 7339 (Toni Technik GmbH)
- Dilatometer L75/30C: thermal expansion measurements
of building materials at constant temperature or during variation of temperature
- DCA-measuring instrument
for the determination of the heat of hydration at cements
- DSC Q200
Measuring instrument for most exact heat flow measurements
- SDT Q600
Simultaneous differential thermal analysis SDT (DSC-TGA): simultaneous measurement of the change of mass (TGA) and of the heat flow (DSC)
from ambient temperatures to 1500 °C
- heat flow surface plate equipment for the determination of the
heat conductivity according to DIN 52616 for plate-like inspection pieces
1.4 Chemical analysis
- ICP spectrometer AKTIVA-M with system MARS 5 Xpress
(manufacturer:Fa. HORIBA Jobin Yvon GmbH)
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1.5 Optical testing methods
- Digital microscope Keyence VHX 600 II (2. generation)
(manufacturer: Fa. Keyence)
1.6 Non destructive testing methods
- BP 7, ultrasonic measuring instrument
(manufacturer: Steinkamp) to the measurement of ultrasonic on times
- ultrasonic measuring instruments
manufacturer Krompholz for the execution of laboratory and building site measurements,
determination of sound on times, computation of flexible constants
(e- and g-modulus, transverse extension coefficient) as well as execution of signal analyses
- Ultrasonic-Tomograph A 1040 Polygon /MIRA
of the company Acoustic Control Systems Ltd.
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Laser measuring technique (photo:
Chr. Meyer)
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- Laser Vibrometer PSV 300 F (company Polytec) with
a high performance
scan head with integrated video system and motorized swiveling tilting head
for the recording of surface oscillations (e.g. natural oscillations of building parts)
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exitation laser (GSI LUMONICS) and scanner (POLYTEC) for the execution of a contactless
measuring method
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Grindo-Sonic/type MK 5 (manufacturer:J. W. Lemmers) conduction of measurement of
self-vibrations (impulse, excitation technique); determination
of elastic constants (E- and G-modulus, poisson‘s ratio)
- EG-meter/model DIGI-EG
c2 (manufacturer: Labek) to the measurement of the resonant frequency, computation
of flexible constants (e- and g-modulus, transverse extension coefficient)
- Georadar test system SIR 3000 of the company GSSI
- Potential field measuring instrument CANIN+ with rod and wheel electrode (Proceq)
- Ferroscan PS 200 of the company HILTI
- Ultrasonic transmitter CELplus
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1.7 Instruments and equipment for the examination of concrete, binders and mortars
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Climate simulation chamber (photo:
Chr. Meyer)
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- CDF/CIF--testing chambers. Cyclic freezing-thawing-demand.
- building materials testing chamber
VB + 03/500 (manufacturer: Heraeus-Vötsch)
- 4 climatic testing equipment for
the simulation of temperature and humidity changes
for investigations of building materials (co-operation between the FIB
and the company Feutron Klimasimulation Greiz/Thuringia)
- Glove-Box GB 2201 (Fisher Scientific GmbH) to working
in CO2-free atmosphere
- Tearing framework (a development of the TU Munich,
Professor Springenschmid) to the determination of the tearing inclination of concrete
- viscosity measuring instrument
VISCO-CORDER (manufacturer: Brabender, Duisburg) for the mortar testing
- BML-viskosimeter (manufacturer: Co
Tec, Reykjavik) [ loan of the ready-mix concrete industry ]
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Tearing framework (photo:
Chr. Meyer)
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- automatic compressive
and bending testing equipment TONICOMP III with vibration table according to DIN EN 196
(manufacturer: TONI-Technik Berlin)
- testing device TIRATEST
24100 for strength investigations (manufacturer: TIRA Maschinenbau GmbH, Rauenstein)
- compressive and bending testing equipment
EDBU 400 for building materials of arbitrary size (manufacturer: Werkstoffprüfung
Heckert, Leipzig)
- Universal test equipment Z 250
(manufacturer: companies Zwick) to the examination of the compressive strength, bending tensile strength and tensile strength up to a breaking load of 250 kN
- servo-hydraulic test equipment
PSB 500/2b (manufacturer: Schenck)
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Universal test equipment Z 250
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- soft imaging system (manufacturer:
SIS GmbH Münster) with transmitted light microscope JENAVERT (manufacturer: Carl Zeiß
Jena) and scanning-table EK 8B. Characterisation of air void systems
in building materials as well as counting of clinker minerals,
also for the determination of the content of mineral admixtures
2008 took place an extension of the measuring technique for the determination of the air void characteristic values at
the hardened concrete in accordance with DIN EN 480-11 (investigation both of thin sections and of polished sections is possible)
- Laser scanning microscope with microfocus
sensor (manufacturer: UBM Meßtechnik GmbH) with triangulation sensor OTM-3-10/F/R
for roughness measurements, e.g. of concrete surfaces
- water impermeability testing set
with qualitative and quantitative recording of measurement (manufacturer: Testing
Bluhm und Feuerherdt) to the determination of the water impermeability
in accordance with DIN 1048
- equipment for the determination
of the gas permeability
- measuring form (self-made) to the continuous determination
of the length variation behavior with inductive displacement
recorder with simultaneous processing of the measured values in the on-line operation
- test framework (self-made) to the continuous determination
of the expansive strength with simultaneous processing of the
measured values in the on-line operation
1.8 Instruments and equipment of the professorship polymer materials
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Particle Charge Detector
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- FT-IR microscope Nicolet iN10 with externalFT-IR module iZ10 (manufacturer: Fa. Thermo Scintific)
- DCA ToniCal Trio (Fa. ToniTechnik)
- pH ION meter pMX (manufacturer: WTW)
- DT 1200
Measuring instrument for the determination of the particle size and the zeta potential of highly concentrated suspensions and emulsions
- Tensiometer K 100
Equipment for the precision measurement of interface tensions and surface tensions
- SPECORD 250
high performance, computer controlled two-radiation spectral photometer among other things
for the determination of degrees of adsorption of polymers with basic studies to the microstructure formation in PCC
- equipment for the determination of adhesive strength
F 15 D Easy M (manufacturer: Freundl Wenningsen) to the determination of adhesive strength
in the measuring range 0... 15 kN
- measuring instrument for the determination of adhesive strength - F 15 D EASY M 2000
- Vibration polishing equipment VibroMet 2
- Particle Charge Detector (PCD)
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2.
Technical equipment for construction-site service, sample production and preparation
- drilling equipment for
core drilling from 50 to 250 mm in diameter in the laboratory and at buildings
- drilling equipment HILTI for
drillings of boreholes with a diameter smaller 50 mm (wet) in the laboratory and at buildings
- rigid endoscope
(visual field angle 67 °) with video recording for the investigation
of the structure of brick-work
- table stone saw STM
90 V, saw blade 900 mm in diameter for the production of test samples
- table stone saw STM
40 St, saw blade 400 mm in diameter for the production of test samples
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Infrared thermometer AMiR 7814-20S
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- precision surface grinding machine
MPS-E 200 for the production of test samples with flat-parallel surfaces
(manufacturer: GMN Georg Müller, Nürnberg)
- cut-off grinding machine/micro saw
WOCU 120 FU for the production of samples of smallest thickness
- grinding and polishing machine
for the production of polished sections among other things for the incident-ligth microscopy
- Infrared thermometer AMiR 7814-20S
Temperature range -30 °C to 900 °C; Accuracy 0.75% of the measured value
optics (standard optics) 60: 1 (19 mm measuring spot with 1,5 m object distance)
optics (close focus) 50 : 1 (6 mm measuring spot with 0,3 m object distance)
operating temperature 0 to 50 °C
- Circulating air drying chamber Heraeus LUT 6050 F
- Ultrasonic bath Sonorex RK 514
- Hand lever knee press APK T-3-40 with different caster knifes
- Compressive filtration equipment
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3. Other
equipment
- systematic line concrete investigations
(manufacturer: TONI-Technik Berlin)
- counter jet pulverizer type
Typ 100 AFG for the production of micro-fine granulations (manufacturer: Alpine)
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Laboratory mixer beba B3
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- plowshare mixer FM 50
(manufacturer: Gebr. Lödige Paderborn) for the homogenization of fine-disperse
materials in the batch process up to approx. 30 kg
- beba B3 laboratory mixer
outstanding mixture results.
The mixing capacity amounts to with a total volume from 1 litre to 2 litres
- concrete calorimeter (self-'s building)
- gradient furnace SO 498 among other things
for burning ceramic materials
- laboratory gradient furnace (self-'s building)
among other things to burning cement raw meals under exactly defined temperature conditions
- programmable climatic test cabinets, types MPC F 25/A25-180
and Weiss SB 11 with moistening and temperature control
within the range 5 .. 95 % r.h. and -25 ... +180 °C
- various mortar and
concrete mixing units
- various balances of different
measuring accuracy for air and underwater weighing
- equipment for production
and for the application of injection foam mortar
- dew point probe MTR 2.2/SL
with Pt 100 (manufacturer: IL-METRONIC Ilmenau) for the execution of dew point measurements
in brick-work drillings up to a depth of 100 cm,
computation of the relative air humidity, recording of the
measured values with data logger (manufacturer: Ahlborn)
- pendulum ram impact testing machine PSW 50
for the determination of the notching work resulting from impact of metallic building materials, plastics
and wood in the capacity range 0... 50 joules
- pendulum ram impact testing machine PSW 300
for the determination of the notching work resulting from impact of metallic building materials, plastics
and wood in the capacity range 0... 300 joules
- equipment for the determination of the hardness
according to the methods Brinell, Rockwell, Vickers
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